Evaluation of Polydimethylsiloxane-Phenylsiloxane as a Coating for Stir Bar Sorptive Extraction

Authors

  • Yamile Pérez-Padilla Cuerpo Académico de Química Fundamental y Aplicada, Facultad de Ingeniería Química, Universidad Autónoma de Yucatán
  • Saúl Ariel Medina Cetina Cuerpo Académico de Química Fundamental y Aplicada, Facultad de Ingeniería Química, Universidad Autónoma de Yucatán
  • Alejandro Ávila-Ortega Cuerpo Académico de Química Fundamental y Aplicada, Facultad de Ingeniería Química, Universidad Autónoma de Yucatán
  • Jesús Alberto Barrón-Zambrano Cuerpo Académico de Química Fundamental y Aplicada, Facultad de Ingeniería Química, Universidad Autónoma de Yucatán
  • Alfredo Rafael Vilchis-Néstor Centro Conjunto de Investigación en Química Sustentable UAEM-UNAM
  • Cristian Carrera-Figueiras Cuerpo Académico de Química Fundamental y Aplicada, Facultad de Ingeniería Química, Universidad Autónoma de Yucatán
  • David Muñoz Rodríguez Cuerpo Académico de Química Fundamental y Aplicada, Facultad de Ingeniería Química, Universidad Autónoma de Yucatán http://orcid.org/0000-0002-6606-3835

DOI:

https://doi.org/10.29356/jmcs.v62i2.431

Keywords:

Sol-gel, polydimethylsiloxane, coating, SBSE, polyaromatics, furanics, antibiotics

Abstract

Analytical pretreatment has become environmental-friendly because of material science assistance. In stir bar sorptive extraction (SBSE), a coating is typically used to isolate and preconcentrate organic compounds in aqueous samples. Here, a translucent coating based on polydimethylsiloxane and phenyltriethoxysilane was prepared by a sol-gel method. Characterization tests showed that the coating was homogeneous, relatively polar, and both thermally (< 400 °C) and chemically stable. Coated stir bars were evaluated in the SBSE experiments. Benzene derivatives were successfully extracted/preconcentrated from aqueous solutions and environmental waters. Furanic derivatives and antibiotics were moderately extracted from water, but they were extracted from isooctane.

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Published

2018-06-06

Issue

Vol. 62 No. 2 (2018): Special Issue on “Modern Analytical Chemistry in Interdisciplinary Research”

Section

Regular Articles

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